NPR's Fresh Air recently featured a photographer named Edward Horsford for his high-speed photography work with water balloons, in which he would pop the balloons and then photograph them right after the gory event - all by himself.
He uses background colors that contrast the color of water in motion, and a flash to light up the water.
Samples from his Flickr page (http://www.flickr.com/photos/edwardhorsford/page2/)
He's disabled downloading and directly linking to his photos, so the best I can do is provide links.
http://www.flickr.com/photos/edwardhorsford/5091496980/sizes/l/
http://www.flickr.com/photos/edwardhorsford/5091497952/
http://www.flickr.com/photos/edwardhorsford/4972135214/
Creative Light provides a good technical article on the methods he uses.
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